HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 69057113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69060853 | HCID 69060853 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69057113 | HCID 69057113 | — |
Reaction Steps
The product was prepared analogously to Example 7.1e starting from 2-(4-iodo-2-isopropenylphenoxy)ethanol and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 1.00 g (60% of theoretical); C24H20ClNO2 (M=389.874); calc.: molpeak (M+H)+: 390/392 (Cl); found: molpeak (M+H)+: 390/392 (Cl); Rf value: 0.30 (silica gel, PE/EtOAc 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5359149752fe4fe9ae25f295d69133ae |
| Source note | uspto-grants-2009_09 |