HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 69057539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69061244 | HCID 69061244 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 69057539 | HCID 69057539 | — |
Reaction Steps
The product was prepared analogously to Example 7.1e starting from 1-[2-(2-hydroxyethoxy)-5-iodophenyl]ethanone and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 0.90 g (70% of theoretical); C23H18ClNO3 (M=391.847); calc.: molpeak (M+H)+: 392/394 (Cl); found: molpeak (M+H)+: 392/394 (Cl); Rf value: 0.55 (silica gel, DCM/MeOH 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-e3beffb7993c44f58a147c1307551df9 |
| Source note | uspto-grants-2009_09 |