HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 86601134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 86077028 | HCID 86077028 | — |
| Product | HCID 86601134 | HCID 86601134 | — |
Reaction Steps
The product was prepared analogously to Example 7.1e starting from 2-(2-hydroxyethoxy)-5-iodobenzaldehyde and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 5.53 g (86% of theoretical); C22H16ClNO3 (M=377.820); calc.: molpeak (M+H)+: 378/380 (Cl); found: molpeak (M+H)+: 378/380 (Cl); HPLC-MS: 5.79 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-62ba48c8263646da9766fba79ef8ebb0 |
| Source note | uspto-grants-2009_09 |