HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 57845330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69056791 | HCID 69056791 | — |
| Product | HCID 57845330 | HCID 57845330 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 1-[3-(4-iodo-2-methylphenyl)propyl]-4-methylpiperidine and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 29 mg (9% of theoretical); C29H31ClN2 (M=443.023); calc.: molpeak (M+H)+: 443/445 (Cl); found: molpeak (M+H)+: 443/445 (Cl); HPLC-MS: 8.55 minutes (method A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-962284b13a4b40a1ad3587905919dc93 |
| Source note | uspto-grants-2009_09 |