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HRID734844

反应详情

EQUATION

反应方程式

HRID 734844 的结构方程式

REACTANTS

反应物

3
结构：ClBr
HCID61697

Bromine chloride (BrCl)

BrCl

2 次

结构：Brc1csc(Br)c1
HCID2724560

Thiophene, 2,4-dibromo-

C4H2Br2S

结构：C#Cc1ccc(-c2ccc(Cl)cc2)cn1
HCID57845328

未命名化合物

PRODUCTS

生成物

1
结构：Clc1ccc(-c2ccc(C#Cc3cc(Br)cs3)nc2)cc1
HCID69055435

未命名化合物

PROCEDURE

实验过程

The product was obtained analogously to Example 7.1e starting from 2,4-dibromothiophene and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 0.78 g (50% of theoretical); C17H9BrClNS (M=374.683); calc.: molpeak (M+H)+: 374/376/378 (BrCl); found: molpeak (M+H)+: 374/376/378 (BrCl); HPLC-MS: 7.40 minutes (method B).

WORKUP

后处理

  1. customThe product was obtained analogously to Example 7.1e
  2. custom7.40 minutes (method B)