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HRID734875

反应详情

EQUATION

反应方程式

HRID 734875 的结构方程式

REACTANTS

反应物

2
结构：CC1CCN(CCOc2ccc(I)cc2)CC1
HCID69061017

未命名化合物

结构：C#Cc1ncc(-c2ccc(Cl)cc2)cc1N(C)C
HCID86076949

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCN(CCOc2ccc(C#Cc3ncc(-c4ccc(Cl)cc4)cc3N(C)C)cc2)CC1
HCID57845326

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1 e starting from 1-[2-(4-iodophenoxy)ethyl]-4-methylpiperidine and [5-(4-chlorophenyl)-2-ethynylpyridin-3-yl]dimethylamine. Yield: 34 mg (5% of theoretical); C29H32ClN3O (M=474.037); calc.: molpeak (M+H)+:474/476 (Cl); found: molpeak (M+H)+:474/476 (Cl); HPLC-MS: 5.40 minutes (method D).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1 e
  2. custom5.40 minutes (method D)