HRID735001

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8675

4-Amino-4'-chlorobiphenyl

C12H10ClN

HCID10110

2-Propynoic acid

C3H2O2

PRODUCTS

生成物

HCID86060771

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21584144

Dichloromethane ethanol

C3H8Cl2O

PROCEDURE

实验过程

Prepared analogously to Example 1.1.b. from 4′-chlorobiphenyl-4-ylamine and propynoic acid. Yield: 0.4 g (29.2% of theory); C15H10ClNO (M=255.70); calc.: molecular ion peak (M+H)+: 256/258; found: molecular ion peak (M+H)+: 256/258; Rf value: 0.35 (silica gel, dichloromethane/ethanol 20:1).

WORKUP

后处理

customPrepared analogously to Example 1.1.b