HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 2-(4-iodophenyl)ethyl Methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-(4-Iodophenyl)ethan-1-ol | HCID 3040770 | — |
| Product | 2-(4-iodophenyl)ethyl Methanesulfonate | HCID 86601888 | — |
Reaction Steps
Prepared analogously to Example 1.2.b. from 2-(4-iodophenyl)ethanol and methanesulfonic acid chloride. Yield: 5.7 g (77.4% of theory); C9H11IO3S (M=326.15); calc.: molecular ion peak (M)+: 326; found: molecular ion peak (M)+: 326.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c86c91840cf64a11936104102b145a56 |
| Source note | uspto-grants-2009_09 |