HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 28948681, compound → HCID 57845828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 28948681 | HCID 28948681 | — |
| Reactant | (2-Chloro-4-trifluoromethylphenyl)propynoic acid | HCID 68817422 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 57845828 | HCID 57845828 | — |
Reaction Steps
Prepared analogously to Example 2.3.f. from 4-(2-pyrazol-1-ylethoxy)phenylamine and (2-chloro-4-trifluoromethylphenyl)propynoic acid. Yield: 56 mg (43% of theory); melting point: 120° C.-125° C.; C21H15ClF3N3O2 (M=433.82); calc.: molecular ion peak (M+H)+: 434/436; found: molecular ion peak (M+H)+: 434/436; Rf value: 0.6 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-f0e87eef6e914bedaaeac233980234b3 |
| Source note | uspto-grants-2009_09 |