HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-(2-diethylaminoethoxy)phenylamine → HCID 57845845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-(2-diethylaminoethoxy)phenylamine | HCID 16791676 | — |
| Reactant | Ammonia methanol dichloromethane | HCID 21584172 | — |
| Reactant | Biphenyl-4-ylpropynoic acid chloride | HCID 86070401 | — |
| Product | HCID 57845845 | HCID 57845845 | — |
Reaction Steps
Prepared analogously to Example 4.1.d. from biphenyl-4-ylpropynoic acid chloride and [2-(2-chloro-4-aminophenoxy)ethyl]diethylamine. Yield: 0.28 g (31.3% of theory); melting point: 105° C.-108° C.; C27H27ClN2O2 (M=446.98); calc.: molecular ion peak (M+H)+: 447/449; found: molecular ion peak (M+H)+: 447/449; Rf value: 0.5 (silica gel, dichloromethane/methanol/ammonia (9:1:0.1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-046cfb0860694ad4b776b0332256add1 |
| Source note | uspto-grants-2009_09 |