HRID735091

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10283

Phenol, 3-chloro-4-nitro-

C6H4ClNO3

HCID13363

1-Chloro-2-(diethylamine)ethane hydrochloride

C6H15Cl2N

PRODUCTS

生成物

HCID68816613

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 4.1.a. from 3-chloro-4-nitrophenol and (2-chloroethyl)diethylamine hydrochloride. Yield: 1.25 g (79.5% of theory); C12H17ClN2O3 (M=272.73); calc.: molecular ion peak (M+H)+: 273/275; found: molecular ion peak (M+H)+: 273/275; Rf value: 0.44 (silica gel, dichloromethane/methanol (90:10)).

WORKUP

后处理

customPrepared analogously to Example 4.1.a