HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane methanol → 3-Bromo-4-(2-diethylaminoethoxy)phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | HCID 68817905 | HCID 68817905 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Bromo-4-(2-diethylaminoethoxy)phenylamine | HCID 59691676 | — |
Reaction Steps
Prepared analogously to Example 3.1.b. from 1.10 g (3.47 mmol) of [2-(2-bromo-4-nitrophenoxy)ethyl]diethylamine in ethyl acetate. Yield: 0.58 g (58% of theory); C12H19BrN2O (M=287.202); calc.: molecular ion peak (M+H)+: 287/289; found: molecular ion peak (M+H)+: 287/289; Rf value: 0.30 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-4f0853a3a21c47f9b9d95f23389d6e0d |
| Source note | uspto-grants-2009_09 |