HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Prolinol → HCID 68817390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Prolinol | HCID 640091 | — |
| Reactant | 1-(2-Bromoethoxy)2-methoxy-4-nitrobenzene | HCID 12937254 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 68817390 | HCID 68817390 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and (S)-1-pyrrolidin-2-ylmethanol. Yield: 0.2 g (25% of theory); C14H20N2O5 (M=296.32); calc.: molecular ion peak (M+H)+: 297; found: molecular ion peak (M+H)+: 297; Rf value: 0.55 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-2fe2b5f1bb964c4ba3947ca1d15fcd4c |
| Source note | uspto-grants-2009_09 |