HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 22185398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 1-(2-Bromoethoxy)2-methoxy-4-nitrobenzene | HCID 12937254 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 22185398 | HCID 22185398 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and morpholine. Yield: 0.3 g (39.4% of theory); C13H18N2O5 (M=282.29); calc.: molecular ion peak (M+H)+: 283; found: molecular ion peak (M+H)+: 283; Rf value: 0.6 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d66bb6bcccd94e8cb2f989e13ed8832c |
| Source note | uspto-grants-2009_09 |