HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22185398, compound → HCID 22185405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22185398 | HCID 22185398 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 22185405 | HCID 22185405 | — |
Reaction Steps
Prepared analogously to Example 3.1.b. from 4-[2-(2-methoxy-4-nitrophenoxy)ethyl]morpholine. Yield: 0.23 g (85.8% of theory); C13H20N2O3 (M=252.31); calc.: molecular ion peak (M+H)+: 253; found: molecular ion peak (M+H)+: 253; Rf value: 0.5 (silica gel, dichloromethane/methanol (9:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-94ebb71a274e4e3fbb6d2539dae244f4 |
| Source note | uspto-grants-2009_09 |