Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclopropanemethanamine → Cyclopropylmethyl-[2-(2-methoxy-4-nitrophenoxy)ethyl]methylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclopropanemethanamine | HCID 75646 | — |
| 반응물 | 1-(2-Bromoethoxy)2-methoxy-4-nitrobenzene | HCID 12937254 | — |
| 반응물 | Dichloromethane methanol | HCID 21226129 | — |
| 생성물 | Cyclopropylmethyl-[2-(2-methoxy-4-nitrophenoxy)ethyl]methylamine | HCID 68816696 | — |
반응 단계
Prepared analogously to Example 1.1.c. from 1 g (3.62 mmol) of 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and 900 mg (10.57 mmol) of cyclopropylmethylamine. Yield: 0.95 g (94% of theory); C14H20N2O4 (M=280.32); calc.: molecular ion peak (M+H)+: 281; found: molecular ion peak (M+H)+: 281; Rf value: 0.4 (silica gel, dichloromethane/methanol (9:1)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07592373B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-858480f0097245f98173d769349eb961 |
| 출처 메모 | uspto-grants-2009_09 |