HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-bromobiphenyl-4-yl)propynoic Acid → 3-(3-Bromobiphenyl-4-yl)propynoic acid-[3-chloro-4-(2-pyrrolidin-1-ylethyl)phenyl]amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-bromobiphenyl-4-yl)propynoic Acid | HCID 68818231 | — |
| Reactant | 3-Chloro-4-(2-pyrrolidin-1-ylethyl)phenylamine | HCID 68818430 | — |
| Product | 3-(3-Bromobiphenyl-4-yl)propynoic acid-[3-chloro-4-(2-pyrrolidin-1-ylethyl)phenyl]amide | HCID 57845810 | — |
Reaction Steps
Prepared analogously to Example 2.3.f. from (3-bromobiphenyl-4-yl)propynoic acid and 3-chloro-4-(2-pyrrolidin-1-ylethyl)phenylamine. Yield: 140 mg (27.2% of theory); C27H24BrClN201 (M=507.84); calc.: molecular ion peak (M+H)+: 507/09/11; found: molecular ion peak (M+H)+: 507/09/11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5d4344d3629d455fb5efa30dabadbe67 |
| Source note | uspto-grants-2009_09 |