HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178489137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | (3-Chloro-2-fluorophenyl)-(4-methoxyphenyl)-methanone | HCID 11471075 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 178489137 | HCID 178489137 | 90.6% |
Reaction Steps
Prepared as in Example 104 from (3-chloro-2-fluoro-phenyl)-(4-methoxy-phenyl)-methanone (0.84 g, 3.2 mmol), hydrazine hydrate (1.0 mL, 32 mmol) and DMAP (0.39 g, 3.2 mmol) to give the product (0.75 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592363B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-8e3576215c0b4dd98d39fcd1a85857dd |
| Source note | uspto-grants-2009_09 |