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HRID73548

反应详情

EQUATION

反应方程式

HRID 73548 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1cnccc1Cl
HCID2735781

4-Chloro-3-nitropyridine

C5H3ClN2O2

结构：CC(C)(C)OC(=O)N[C@@H]1CNC[C@H](CO[Si](C)(C)C(C)(C)C)C1
HCID131729686

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@H]1C[C@@H](CO[Si](C)(C)C(C)(C)C)CN(c2ccncc2[N+](=O)[O-])C1
HCID131729685

未命名化合物

PROCEDURE

实验过程

Method 1 was followed using cis (+/−)-tert-butyl 5-((tert-butyl-dimethylsilyloxy)methyl)piperidin-3-ylcarbamate and 4-chloro-3-nitropyridine yielding cis (+/−)-tert-butyl 5-((tert-butyldimethylsilyloxy)methyl)-1-(3-nitropyridin-4-yl)-piperidin-3-ylcarbamate. LCMS (m/z): 467.0 (MH+); LC Rt=4.02 min.