HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitro-2-(propane-2-sulfonyl)benzonitrile → 5-Amino-2-(isopropylsulfonyl)benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitro-2-(propane-2-sulfonyl)benzonitrile | HCID 57448206 | — |
| Reactant | 5-Amino-2-(ethanesulfonyl)benzonitrile | HCID 59838037 | — |
| Product | 5-Amino-2-(isopropylsulfonyl)benzonitrile | HCID 57448207 | 95.3% |
Reaction Steps
Using a procedure analogous to that used to prepare 6B, 9A (632 mg, 2.48 mmol) was hydrogenated to give 9B (530 mg, 95%) as a white solid. MS (ESI) m/z 225.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-df4243df72bb43089280543f706b9655 |
| Source note | uspto-grants-2009_09 |