4-Aminobenzonitrile → HCID 68818316, compound

Participants

Reaction Steps

Using a procedure analogous to that used to prepare 2D, 15C (0.101 g, 0.20 mmol) was reacted with 4-aminobenzonitrile (0.024 g, 0.2 mmol) and glyoxylic acid monohydrate (0.018 g, 0.2 mmol) to give, after purification by reverse phase HPLC, 15D (78 mg, 62%) as a white solid. MS (ESI) m/z 634.9 (M+H)+.

Provenance & Evidence