3-Aminobenzamide → HCID 57842648, compound

Participants

Reaction Steps

Using a procedure analogous to that used to prepare 2D, 16I (0.134 g, 0.25 mmol) was reacted with m-aminobenzamide (0.035 g, 0.26 mmol) and glyoxylic acid monohydrate (0.023 g, 0.25 mmol) to give, after purification by reverse phase HPLC, 16J (134 mg, 78%) as a pale yellow foam. MS (ESI) m/z 683.1 (M+H)+.

Provenance & Evidence