HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59838042, compound → HCID 59838059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59838042 | HCID 59838042 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59838059 | HCID 59838059 | — |
Reaction Steps
A mixture of 19G (77 mg, 0.14 mmol), 20% palladium(II) hydroxide on carbon (94 mg) and ethanol (20 mL) was hydrogenated (55 psi) for 4 h. The reaction mixture was filtered and concentrated under reduced pressure to give 19H (47 mg, 90%) as a yellow solid. LC-MS m/z: 378.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d98c8b61ff6b4d44b5bf2cd4cc3046be |
| Source note | uspto-grants-2009_09 |