HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatobenzonitrile → 1-(4-Bromophenethyl)-3-(3-cyanophenyl)-1-methylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatobenzonitrile | HCID 2733315 | — |
| Reactant | 2-(4-Bromophenyl)-N-methylethan-1-amine | HCID 18367556 | — |
| Reactant | 1-(3-(4-Bromophenyl)propyl)-3-(3-cyanophenyl)-1-methylurea | HCID 57842621 | — |
| Product | 1-(4-Bromophenethyl)-3-(3-cyanophenyl)-1-methylurea | HCID 57842819 | 81% |
Reaction Steps
Using a procedure analogous to that used to prepare 22C, 23B (300 mg, 1.4 mmol) was reacted with 3-isocyanatobenzonitrile to yield 23C (406 g, 81%) as a clear oil. MS (ESI) m/z 358.31/360.29 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3bcc7b5769f44f1cb361ed3c3eb6e860 |
| Source note | uspto-grants-2009_09 |