HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzamide → HCID 57842780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzamide | HCID 1645 | — |
| Reactant | Glyoxylic acid, monohydrate | HCID 15620607 | — |
| Reactant | 4-(2-((Benzyloxycarbonyl)(methyl)amino)ethyl)phenylboronic acid | HCID 57842578 | — |
| Product | HCID 57842780 | HCID 57842780 | 76% |
Reaction Steps
Using a procedure analogous to that used to prepare 2D, 28D (400 mg, 1.3 mmol) was reacted with 3-aminobenzamide and glyoxylic acid monohydrate to afford 28E (661 mg, 76%) as a yellow solid. MS (ESI) m/z 462.32 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-70fb0faa064d4952ab71e83adf247fe3 |
| Source note | uspto-grants-2009_09 |