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HRID735580

反应详情

EQUATION

反应方程式

HRID 735580 的结构方程式

REACTANTS

反应物

2
结构：CCS(=O)(=O)c1ccc(NC(=O)N(C)CCc2ccc(C(Nc3ccc4c(N(C(=O)OC(C)(C)C)C(=O)OC(C)(C)C)nccc4c3)C(=O)O)cc2)cc1CN
HCID57842775

未命名化合物

结构：Cc1cc(C(Nc2ccc3c(N(C(=O)OC(C)(C)C)C(=O)OC(C)(C)C)nccc3c2)C(=O)O)ccc1CCOC(=O)Nc1cccc(C#N)c1
HCID57956367

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C(Nc2ccc3c(N(C(=O)OC(C)(C)C)C(=O)OC(C)(C)C)nccc3c2)C(=O)O)ccc1CCOC(=O)Nc1cccc(CN)c1
HCID57956364

未命名化合物

收率 45.5%

PROCEDURE

实验过程

Using a procedure analogous to that used to prepare 25E, 30E (308 mg, 0.44 mmol) was hydrogenated for 15 h and purified by reverse phase HPLC to give 30F (140 mg, 45%) as a yellow solid. MS (ESI) m/z 700.15 (M+H)+.

WORKUP

后处理

  1. custompurified by reverse phase HPLC