HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-dimethylphenethyl 3-cyano-4-(ethylsulfonyl)phenylcarbamate → HCID 57842551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-dimethylphenethyl 3-cyano-4-(ethylsulfonyl)phenylcarbamate | HCID 57842545 | — |
| Reactant | 4-(4-(3-Cyano-4-(ethylsulfonyl)phenylamino)-4-oxobutyl)phenylboronic acid | HCID 57842684 | — |
| Product | HCID 57842551 | HCID 57842551 | 54% |
Reaction Steps
Using a procedure analogous to that used to prepare 6D, 32C (480 mg, 1.0 mmol) was reacted with 5,5′,5′-tetramethyl-[2,2′]bi[[1,3,2]dioxaborinanyl] to give 32D (240 mg, 54%) as a tan solid. MS (ESI) m/z 453.12 (M+Na)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-605ff3cf5c9641aebb1d69e8360345ce |
| Source note | uspto-grants-2009_09 |