HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzamide → HCID 57842901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzamide | HCID 1645 | — |
| Reactant | Glyoxylic acid, monohydrate | HCID 15620607 | — |
| Reactant | 4-(2-(Tert-butyldimethylsilyloxy)ethyl)-3-ethylphenylboronic acid | HCID 57842608 | — |
| Product | HCID 57842901 | HCID 57842901 | 88% |
Reaction Steps
Using a procedure analogous to that used to prepare 2D, 46B (1.4 g, 4.1 mmol) was reacted with 3-aminobenzamide and glyoxylic acid monohydrate to afford 46C (1.25 g, 88%) as a yellow solid. MS (ESI) m/z 343.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c18860a9465d4d698a78b052b5065817 |
| Source note | uspto-grants-2009_09 |