HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzonitrile → 4-(4-bromo-2-methylphenyl)-N-(3-cyanophenyl)butanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzonitrile | HCID 16702 | — |
| Reactant | 4-(4-Bromo-2-methylphenyl)butanoic acid | HCID 57842616 | — |
| Reactant | 4-(4-Bromophenyl)-N-(3-cyano-4-(ethylsulfonyl)phenyl)butanamide | HCID 57842667 | — |
| Product | 4-(4-bromo-2-methylphenyl)-N-(3-cyanophenyl)butanamide | HCID 57842745 | 76% |
Reaction Steps
Using a procedure analogous to that used to prepare 6C, 55B (216 mg, 0.84 mmol) was reacted with 3-aminobenzonitrile to afford 55C (228 mg, 76%) as a solid. MS (ESI) m/z 358.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-8c54c5559cff455db3643cff6f0ef84f |
| Source note | uspto-grants-2009_09 |