HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isocyanatobenzonitrile → HCID 68817589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isocyanatobenzonitrile | HCID 2733315 | — |
| Reactant | 2-(4-Bromo-2-ethylphenyl)ethanol | HCID 57842784 | — |
| Reactant | 4-Bromo-2-methylphenethyl 3-cyanophenylcarbamate | HCID 57842847 | — |
| Product | HCID 68817589 | HCID 68817589 | 57% |
Reaction Steps
Using a procedure analogous to that used to prepare 30C, 36B (687 mg, 3 mmol) was reacted with 3-isocyanatobenzonitrile (432 mg, 3 mmol) to give 56A (630 mg, 57%) as an oil. MS (ESI) m/z 373.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-c59c64fc60c54d72b6c01ed3791935bd |
| Source note | uspto-grants-2009_09 |