HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57842704, compound → (S)-4-(2-(3-(1-(benzyloxycarbonylamino)ethyl)phenylcarbamoyloxy)ethyl)-3-methylphenylbromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57842704 | HCID 57842704 | — |
| Reactant | (S)-benzyl 1-(3-aminophenyl)ethylcarbamate | HCID 57842795 | — |
| Reactant | 2-(4-Bromo-2-methylphenyl)ethanol | HCID 57842852 | — |
| Product | (S)-4-(2-(3-(1-(benzyloxycarbonylamino)ethyl)phenylcarbamoyloxy)ethyl)-3-methylphenylbromide | HCID 57842764 | 9% |
Reaction Steps
Using a procedure analogous to that used to prepare 34D, 59B (1.5 g 5.5 mmol) was reacted with 30B to give 59C (2.46 g, 9%) as an oil. MS (ESI) m/z 512.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-7e5b5a279a1446b8ad9751748742fc21 |
| Source note | uspto-grants-2009_09 |