HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57842704, compound → 4-(2-(3-(((Benzyloxycarbonyl)(methyl)amino)methyl)phenylcarbamoyloxy)ethyl)-3-methylphenylbromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57842704 | HCID 57842704 | — |
| Reactant | 2-(4-Bromo-2-methylphenyl)ethanol | HCID 57842852 | — |
| Reactant | Benzyl 3-aminobenzyl(methyl)carbamate | HCID 57842860 | — |
| Product | 4-(2-(3-(((Benzyloxycarbonyl)(methyl)amino)methyl)phenylcarbamoyloxy)ethyl)-3-methylphenylbromide | HCID 57842874 | 69% |
Reaction Steps
Using a procedure analogous to that used to prepare 34D, 60B (1.6 g, 5.9 mmol) was reacted with 30B to give 60C (2.0 g, 69%) as an oil. MS (ESI) m/z 512.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-1c0c1f234e2a4594ba8ebfc000aadf8d |
| Source note | uspto-grants-2009_09 |