Ethanol → HCID 57842769, compound

Participants

Reaction Steps

To a refluxing solution of 64A (5 g, 16.7 mmol), EtOH (100 mL), water (30 mL) and AcOH (15 mL) was added portion-wise Fe powder (5 g, 89 mmol) over 30 min. The mixture was heated for 1 h. before cooling to ambient temperature. and filtering through celite. The filtrate was concentrated in vacuo to afford 64B (2.7 g, 61%) as an oil. MS (ESI) m/z 271.2 (M+H)+.

Provenance & Evidence