HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57842873, compound → HCID 57842887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57842873 | HCID 57842873 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57842887 | HCID 57842887 | 67.1% |
Reaction Steps
To a solution of 68C (160 mg) in 10 mL MeOH, was added Pd/C (50 mg). The mixture was hydrogenated at 60 psi for 60 min. The mixture was filtered, concentrated and purified by flash chromatography (0 to 15% MeOH in DCM) to give 68D (108 mg, 66%). MS (ESI) m/z 706.3(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-54eb1b31f3e84772870134a07b8aeff2 |
| Source note | uspto-grants-2009_09 |