HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-(4-Bromophenyl)propan-2-yloxy)(tert-butyl)dimethylsilane → 4-(2-(Tert-butyldimethylsilyloxy)propyl)phenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-(4-Bromophenyl)propan-2-yloxy)(tert-butyl)dimethylsilane | HCID 57842700 | — |
| Reactant | 4-(1-(Tert-butyldimethylsilyloxy)propan-2-yl)phenylboronic acid | HCID 57842782 | — |
| Product | 4-(2-(Tert-butyldimethylsilyloxy)propyl)phenylboronic acid | HCID 57842803 | 54% |
Reaction Steps
According to the procedure for the preparation of 73D, 77B (2.14 g, 6.50 mmol) afforded 1.04 g (54%) of 77C as a colorless solid. MS (ESI) m/z 295.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592331B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3c3399616370472a94e8146731f45c42 |
| Source note | uspto-grants-2009_09 |