HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 4-(hexyloxy)- → Ethyl[benzyl(4-{[4-(hexyloxy)benzoyl]amino}benzyl)amino]-(oxo)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 4-(hexyloxy)- | HCID 170235 | — |
| Reactant | Ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate | HCID 67187687 | — |
| Product | Ethyl[benzyl(4-{[4-(hexyloxy)benzoyl]amino}benzyl)amino]-(oxo)acetate | HCID 67186531 | 58% |
Reaction Steps
The same procedure as employed in the preparation of Example 15, step d but using 4-hexyloxy-benzoyl chloride and ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate gave the title compound as a colorless oil (58%). M−(ESI): 515.2. HPLC (Condition A), Rt: 6.0 min (HPLC purity: 94.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-e526092712d24841b39530a47b3d5632 |
| Source note | uspto-grants-2009_09 |