HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetradec-9-enoyl chloride → HCID 67187061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetradec-9-enoyl chloride | HCID 54048966 | — |
| Reactant | HCID 67187634 | HCID 67187634 | — |
| Product | HCID 67187061 | HCID 67187061 | 81% |
Reaction Steps
The same procedure as employed in the preparation of Example 15, step d using ethyl{(4-aminobenzyl)[4-(trifluoromethyl)benzyl]amino}(oxo)acetate and tetradec-9-enoyl chloride gave the title compound as a colorless oil (81%). M−(LC/MS(ESI)): 588.0. HPLC (Condition A), Rt: 7.3 min (HPLC purity: 96.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-037e902e932f43209589603b8d5c765d |
| Source note | uspto-grants-2009_09 |