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HRID735886

反应详情

EQUATION

反应方程式

HRID 735886 的结构方程式

REACTANTS

反应物

2
结构：NCc1ccc(C(F)(F)F)cc1
HCID76804

4-(Trifluoromethyl)benzylamine

C8H8F3N

结构：CCCCCCCCCCCCNC(=O)c1ccc(C(C)=O)cc1
HCID67186598

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCNC(=O)c1ccc(C(C)NCc2ccc(C(F)(F)F)cc2)cc1
HCID67186177

未命名化合物

收率 71%

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 223 (step b) but using 4-acetyl-N-dodecylbenzamide and 4-(trifluoromethyl)benzylamine gave the title compound as a colorless oil (71%). M−(LC/MS(ESI)): 489.1; M+(LC/MS(ESI)): 491.5. HPLC (Condition A), Rt: 5.51 min (HPLC purity: 50.0%).

WORKUP

后处理

  1. customThe same procedure as employed in the preparation of Example 223 (step b)