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HRID735891

反应详情

EQUATION

反应方程式

HRID 735891 的结构方程式

REACTANTS

反应物

2
结构：NCc1ccc([N+](=O)[O-])cc1
HCID29147

4-Nitrobenzylamine

C7H8N2O2

结构：O=C(c1ccc(C(F)(F)F)cc1)C1CCCC1
HCID24724174

Cyclopentyl[4-(trifluoromethyl)phenyl]methanone

C13H13F3O

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(CNC(c2ccc(C(F)(F)F)cc2)C2CCCC2)cc1
HCID67186505

未命名化合物

收率 67%

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 223 (step b) but using cyclopentyl[4-(trifluoromethyl)phenyl]methanone and 4-nitrobenzylamine gave the title compound as an oil (67%). M−(LC/MS(ESI)): 377.2; M+(LC/MS(ESI)): 379.2

WORKUP

后处理

  1. customThe same procedure as employed in the preparation of Example 223 (step b)