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HRID735911

反应详情

EQUATION

反应方程式

HRID 735911 的结构方程式

REACTANTS

反应物

2
结构：CC(N)c1ccc(C(F)(F)F)cc1
HCID2782449

1-(4-Trifluoromethylphenyl)ethylamine

C9H10F3N

结构：CCCCCCCCC#Cc1ccc(C=O)cc1
HCID57841320

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCC#Cc1ccc(CNC(C)c2ccc(C(F)(F)F)cc2)cc1
HCID67189397

未命名化合物

收率 54%

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 226 (step a) but using 4-dec-1-ynylbenzaldehyde and 1-[4-(trifluoromethyl)phenyl]ethanamine gave the title compound as a colorless oil (54%). M+(ESI): 416.2. HPLC (Condition A), Rt: 4.67 min (HPLC purity: 87.6%).

WORKUP

后处理

  1. customThe same procedure as employed in the preparation of Example 226 (step a) but