N-Methyl-D-glucamine → HCID 69001242, compound

Participants

Reaction Steps

The same procedure as employed in the preparation of Example 2 but using N-methyl-D-glucamine and {{1-methyl-1-[4-(trifluoromethyl)phenyl]ethyl}[4-(3-undecyl-1,2,4-oxadiazol-5-yl)benzyl]amino}(oxo)acetic acid gave the title compound as a white powder (95%). M−(LC/MS(ESI)): 586.3. HPLC (Condition A), Rt: 6.22 min (HPLC purity: 99.9%). Analysis calculated for C32H40F3N3O4.C7H17NO5▪1.5H2O: C, 57.84; H, 7.47; N, 6.92%. Found: C, 57.79; H, 7.46; N, 6.88%.

Provenance & Evidence