N-Methyl-D-glucamine → HCID 69001639, compound

Participants

Reaction Steps

The same procedure as employed in the preparation of Example 2 but using N-methyl-D-glucamine and {{[4-(dodecyloxy)-1-naphthyl]methyl}[4-(trifluoromethyl)benzyl]amino}(oxo)acetic acid gave the title compound as a pink solid (68%). M−(LC/MS(ESI)): 570.3. HPLC (Condition A), Rt: 6.45 min (HPLC purity: 99.7%). Analysis calculated for C33H40F3NO4.C7H17NO5▪1.5H2O: C, 60.52; H, 7.62; N, 3.53%. Found: C, 60.71; H, 7.50; N, 3.56%.

Provenance & Evidence