4-Nitrobenzaldehyde → HCID 67185728, compound

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Reaction Steps

The same procedure as employed in the preparation of Example 226 (step a) but using 3,5-dichlorobenzylamine and 4-nitrobenzaldehyde gave the title compound as a yellow powder (71%). 1H NMR (CD3OD, 300 MHz) δ 8.37 (d, 2H, J=8.8 Hz), 7.83 (d, 2H, J=8.8 Hz), 7.61 (br s, 3H), 4.48 (s, 2H), 4.38 (s, 2H). M−(LC/MS(ESI)): 309; M+(LC/MS(ESI)): 311 HPLC (Condition A), Rt: 2.78 min (HPLC purity: 93.0%).

Provenance & Evidence