1,3-Benzodioxol-5-amine → HCID 67185714, compound

HRID 735982Notes

Reaction equation

HRID 735982 reaction equation
[CH2:1]([C:12]1[N:16]=[C:15]([C:17]2[CH:18]=[C:19]([CH:22]=[CH:23][CH:24]=2)[CH:20]=O)[O:14][N:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[O:25]1[C:29]2[CH:30]=[CH:31][C:32]([NH2:34])=[CH:33][C:28]=2[O:27][CH2:26]1>>[O:25]1[C:29]2[CH:30]=[CH:31][C:32]([NH:34][CH2:20][C:19]3[CH:22]=[CH:23][CH:24]=[C:17]([C:15]4[O:14][N:13]=[C:12]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[N:16]=4)[CH:18]=3)=[CH:33][C:28]=2[O:27][CH2:26]1

Participants

3

Reactant 2

HCID 843101,3-Benzodioxol-5-amineHCID 865985383-(3-Undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde

Product 1

HCID 67185714HCID 67185714, compound

Procedure

The same procedure as employed in the preparation of Example 357 (step a) but using 3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde and 1,3-benzodioxol-5-ylamine gave the title compound as an oil. M+(LC/MS(ESI)): 450.4. HPLC (Condition A), Rt: 5.12 min (HPLC purity: 95.4%).

Workup

  1. customThe same procedure as employed in the preparation of Example 357 (step a) but

Sources & evidence

ORD record
ord-577301c153534114bd57f1e8217d68b8
Source dataset
uspto-grants-2009_09
Patent number
US07592477B2

Reaction notes

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