3,4-Dichlorophenethylamine → N-(4-dec-1-ynylbenzyl)-N-[2-(3,4-dichlorophenyl)ethyl]amine

Participants

Role	Name	HCID	Charge
Reactant	3,4-Dichlorophenethylamine	HCID 217958	—
Reactant	4-Dec-1-ynylbenzaldehyde	HCID 57841320	—
Product	N-(4-dec-1-ynylbenzyl)-N-[2-(3,4-dichlorophenyl)ethyl]amine	HCID 67189153	—

Reaction Steps

The same procedure as employed in the preparation of Example 394 (step b) but using 4-dec-1-ynylbenzaldehyde and 2-(3,4-dichlorophenyl)ethylamine gave the title compound as an oil. M+(LC/MS(ESI)): 416.3. HPLC (Condition A), Rt: 4.91 min (HPLC purity: 72.4%).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07592477B2
Source dataset	uspto-grants-2009_09
ORD ID	ord-ead9835c5a784717b389bcfe93777fee
Source note	uspto-grants-2009_09