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HRID736000

反应详情

EQUATION

反应方程式

HRID 736000 的结构方程式

REACTANTS

反应物

2
结构：NCCc1ccc(Cl)c(Cl)c1
HCID217958

3,4-Dichlorophenethylamine

C8H9Cl2N

结构：CCCCCCCCCCC#Cc1ccc(C=O)cc1
HCID86598536

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCC#Cc1ccc(CNCCc2ccc(Cl)c(Cl)c2)cc1
HCID67187845

未命名化合物

PROCEDURE

实验过程

The same procedure as employed in the preparation of Example 394 (step b) but using 4-dodec-1-ynylbenzaldehyde and 2-(3,4-dichlorophenyl)ethylamine gave the title compound as an oil. M+(LC/MS(ESI)): 444.4. HPLC (Condition A), Rt: 5.27 min (HPLC purity: 83.9 %).

WORKUP

后处理

  1. customThe same procedure as employed in the preparation of Example 394 (step b)