HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenethylamine → N-[2-(3,4-dichlorophenyl)ethyl]-N-{[4-(dodecyloxy)-1-naphthyl]methyl}amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenethylamine | HCID 217958 | — |
| Reactant | 4-(Dodecyloxy)-1-naphthaldehyde | HCID 85841201 | — |
| Product | N-[2-(3,4-dichlorophenyl)ethyl]-N-{[4-(dodecyloxy)-1-naphthyl]methyl}amine | HCID 67187143 | — |
Reaction Steps
The same procedure as employed in the preparation of Example 394 (step b) but using 4-(dodecyloxy)-1-naphthaldehyde and 2-(3,4-dichlorophenyl)ethylamine gave the title compound as an oil. HPLC (Condition A), Rt: 5.72 min (HPLC purity: 82.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-808fbff75d13439b84e0bf1fcf29576c |
| Source note | uspto-grants-2009_09 |