HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Decyne → HCID 67188441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Decyne | HCID 12997 | — |
| Reactant | HCID 67189049 | HCID 67189049 | — |
| Product | HCID 67188441 | HCID 67188441 | — |
Reaction Steps
The same procedure as employed in the preparation of Example 226 (step c) but using ethyl{(2-bromobenzyl)[4-(trifluoromethyl)benzyl]amino}(oxo)acetate and dec-1-yne gave the title compound as a pale yellow oil. M−(LC/MS(ESI)): 472.0. HPLC (Condition A), Rt: 5.51 min (HPLC purity: 99.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-4ec36e935be74967a2196453374194e8 |
| Source note | uspto-grants-2009_09 |