HCID 68900725, compound → HCID 68903347, compound

Participants

Reaction Steps

Add Pd/C (10%) (470 mg) to a solution of 4-Benzyl-2-{2-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-1-phenyl-ethylidene}-morpholine (470 mg, 0.97 mmol) in 10 ml of MeOH, bubble H2 and stir at room temperature for 4 h. Concentrate the solvent under reduced pressure to give a residue. Purify the residue by column chromatography eluting with CH2Cl2:MeOH 9:1 to afford pure the title compound as colourless oil.

Provenance & Evidence