HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 57559158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Ethyl 8-fluoro-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate | HCID 66639977 | — |
| Product | HCID 57559158 | HCID 57559158 | — |
Reaction Steps
The title compound was prepared in a manner similar to that described in Example 2A by using ethyl 8-fluoro-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate and benzoyl chloride; 1H-NMR (CDCl3): δ 10.57 (1H, br s), 8.05 (1H, s), 7.55 (3H, m), 7.45 (3H, m), 7.05 (1H, dd), 6.87 (1H, m), 4.22 (4H, m), 3.24 (2H, t), 1.2 (3H, t); MS (ES): 379 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595311B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-e2e93b2c92f34d529e339e4f70649d31 |
| Source note | uspto-grants-2009_09 |